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By M. Smith

ISBN-10: 0471145793

ISBN-13: 9780471145790

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Nishio, K. J. Org. ; Srehnik. M. J. Org. , 1995, 60, 3278 In, H20, 30 min „ H ,Br Li. -J. ; Sato. F. ; Sato. F. TMSOTf,CH£l 2 , -78°C 2. Bu3SnCH2CH=CH2 -40°C 3. TBAF (>99 : <1) 98% Kim. H. ; Reisse, ]. ; Das. P. ; Chan. -H. ; Wada, M. Chem. Br 2. ; Sato. F. J. Am. Chem. ; Cohen, T. Synth. , 1995, 25, 33 O "* Q \ """"O PhCHO, 10% PdCPhCN)^ 3 SnCl2»2 HP, DMI, 25°C HQ,, " 91% Rang. -B. Synth. : Wu. -H. Svnth. ; Yamamoto. Y. J. Chem. Soc. Chem. 1 : 9) 48% H2O , BU4NBr (1 : 99) 48% Masuyama. ; Kurusu, Y.

S. , 1993, 34, 7827 R-BINOL/Ti(OiPr)4 , MS 4A , TFA H PhCHO -20°C , 14h , 95% (96% ee) Keck. C. J. Org. , 1993, 58, 6543 Section 36 Alcohols from Amides 15 CC1;£HO, R-BINOL-TiCl2 MS 4A, 0°C , CH2C12 (62 CCb : 38) 78% [>95%ee] CCb [>95%ee] Mikami. ; Uchimaru, T. ; Tagliavini. ; Umani-Ronchi. A. /. Am. Chem. , 1993, 115, 7001 j [ Ti(OiPr)4/l,l'-bi-2-naphthol, MS4A1 I CH2C12, reflux j PhCHO *- -78°C,10min 2. ^^^ SnBu3 , -20°C , 70h 88% (95%ee,R) Keck. S. /. Am. Chem. , 1993, 115, 8467 1. Et2Zn , 25°C, 10% UO#*\,UH OH PhCHO 2.

Prep. Proceed. , 1995, 27, 361 SECTION 26: ACID DERIVATIVES FROM HYDRIDES NO ADDITIONAL EXAMPLES SECTION 27: ACID DERIVATIVES FROM KETONES Na£O3-3/2 H2O2,60°C 3h Yang. W. Synth. , 1995, 25, 3695 SECTION 28: ACID DERIVATIVES FROM NITRILES NO ADDITIONAL EXAMPLES SECTION 29: ACID DERIVATIVES FROM ALKENES , Fe(CO)5, KOH, CO (1 atm) H2O/iPrOH, 55°C, 4d Me (96 : 4) 45% Brunet. S. 8 atm) , DME Pd(OAc)2 - dppb , 150°C , 16h \_ I 86% El AH. : Alper, H. J. Org. , 1993, 58, 3595 D. 8atmCO 10% Pd/C , dppb , DME 150°C,ld (76 : El Ali.

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