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Ar Rx. 3-7 REFERENCES 37. 38: 36222 41. 6123e 45. 67: 108605~ 38. 42: 1209h 42. 56: 5943d 46. 7 9 66254y 39. ss: 114sJd 43. 69. 76826u 40. 45: 2619b 44. 4. 4-l), included some 5-phenyl intermediates (Eq. 39). The yields are generally excellent. Organometallic azides add smoothly to acetylenes (Eqs. 4-3)49derivatives hydrolyze in near quantative yield. 4-4) followed by hydrolysis (Eq. 42)" is another attractive route. 4-5. " Except for Ph and 9-anthryl (SO and 60°/0), the yields are 80 to 90%. 4-6 H Ar = Ph, 4-MeOPh, 4-CIPh.

1,4-Alkyl- or Aryl-Disubstituted lH-1,2,3-Triazoles 4 9 6242c -4-acetaldehyde, I-phenyl-, oxime 1-(2-acetamido-2-deoxy-~-D-glucopyranosyl)-4-phenyl72: 371811 1-(2-acetamido-2-deoxy-~-D-glucopyranosyl)-4-phenyl-, 72: 371th 3',4',6'-triacetate ester - 1-acetic acid, 4(or 5)-(I-hydroxycyclohexy1)-, 60: 15859d ethyl ester - 1-acetic acid, 4(or 5)-(1-hydroxyethy1)-, 60. 15859d ethyl ester - 1-acetic acid, 4-(hydroxy-l-methylethyl)-, 60: 15859d ethyl ester -1-acetic acid, 4-phenyl8 0 108451~ - I-acetic acid, 4(or 5)-phenyl60: 1585W - 1-acetic acid.

Chem.. 119, 173 (1928). A. Quilico, Gazz. Chim. +61, 759 (1931). F. Amdt, H. Scholz, and Frobel, Justus Liebigs Ann. , 521, 95 (1935). S. Fridman and N. Lisovs’ka, Zapiski Inst. , Akad. Nauk URSR, Inst. , 6, 353 (1940). Ghigi and T. Pozzo-Balbi,Gazz. Chim. ItaL 71, 228 (1941). R. Hiittel,Chem. , 74B. 1680 (1941). Wagner-Roemmich,Jushcs Liebigs Ann. , 554, 15 (1943). J. L. Sumrell,J. Org. ,13, 807 (1948). J. C. Sheehan and C. A. Robinson, J. Amer. Chem. , 73, 1207 (1951). J. L. A. Stauffer,J . Org.

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Chemistry of superconductor materials by Vanderah T.A.(ed)


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