By Do D.D.
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Extra info for Adsorption analysis: Equilibria and kinetics
The designated analytical methods are all nondestructive and avoid alterations of the samples that can therefore be further used. Acknowledgements We are most grateful to the ETH Zürich which funded this project. We would also thank Dr. Andreas Wahl from PENNAROYA Oxide who donated to us the lead oxide. Thanks to Dr. Karsten Kunze Geological Institute ETH Zürich and Peter Wägli Laboratory for Solid State Physics ETH Zürich for making the SEM pictures possible. Susan Tandy and Paula Amunátegui we would like to thank for cross-reading the manuscript.
Although common to the different FTIR techniques, factors such as resolution, apodization and zero filling have to be optimized in respect with the physical state of the material to be analyzed. For instance, bandwidths are intrinsically broad in solid state, and there is no need to increase inconsiderately the resolution for DRIFT spectroscopy. Otherwise, the signal to noise ratio of the spectrum will be lowered (according to the trading rules), without gaining further spectral informations. During a previous work (Azambre et al.
It could be shown that the used technique to attach particulate matter onto a support is suitable. 2 Coating Process The coating process itself is not difficult to handle. A constant distance between the dust spray gun and the epoxy covered supports should be used. Also a constant air flow/pressure and a constant spray time should be kept. These are the most favorable conditions to produce polymer supports that are uniformly covered with heavy metal phases. It is self-evident that the application step can only be carried out in rooms with appropriate dust and air extraction units.
Adsorption analysis: Equilibria and kinetics by Do D.D.